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Hydrogen Sulfide → 17beta-Ethylthio-9-fluoro-11beta-hydroxy-17alpha-mercaptoandrosta-1,4-diene-3-one

HRID 543465
ノート
印刷プレビュー

反応式

HRID 543465 の反応式
[CH2:1]([S:3][C:4]1[C@:5]2([CH2:22][C@H:21]([OH:23])[C@@:20]3([F:24])[C@@H:10]([CH2:11][CH2:12][C:13]4[C@:18]3([CH3:19])[CH:17]=[CH:16][C:15](=[O:25])[CH:14]=4)[C@@H:7]2[CH2:8][CH:9]=1)[CH3:6])[CH3:2].[SH2:26].B(F)(F)F.CCOCC>ClCCl.C(Cl)(Cl)Cl>[CH3:2][CH2:1][S:3][C@@:4]1([SH:26])[CH2:9][CH2:8][C@H:7]2[C@H:10]3[C@:20]([F:24])([C@@H:21]([OH:23])[CH2:22][C@:5]12[CH3:6])[C@:18]1([CH3:19])[C:13](=[CH:14][C:15](=[O:25])[CH:16]=[CH:17]1)[CH2:12][CH2:11]3
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

6

反応物 3

HCID 402Hydrogen SulfideHCID 8000Boron trifluoride etherateHCID 1291771217-Ethylthio-9-fluoro-11beta-hydroxyandrosta-1,4,16-triene-3-one

生成物 1

HCID 1327444317beta-Ethylthio-9-fluoro-11beta-hydroxy-17alpha-mercaptoandrosta-1,4-diene-3-one

試薬・触媒・溶媒 2

HCID 6212Chloroform溶媒
HCID 6344
Dichloromethane
溶媒

反応条件

温度
-40 °C

実験手順

A solution of 2.0 g of 17-ethylthio-9-fluoro-11β-hydroxyandrosta-1,4,16-triene-3-one in dry dichloromethane (120 ml) was cooled and stirred in a bath at about -40° C. and a slow stream of hydrogen sulfide gas was passed into the solution while boron trifluoride etherate (1.2 ml) was added. After about 3.5 to 4.0 hours, the mixture was diluted with chloroform, warmed to room temperature and washed successively with a dilute sodium bicarbonate solution and water. The soluiton was dried (anhydrous magnesium sulfate), evaporated and the solid residue crystallized from ethyl acetate to afford 1.4. g of the title compound, melting point 239°-242° C.

後処理

  1. additionwas added
  2. temperaturewarmed to room temperature
  3. washwashed successively with a dilute sodium bicarbonate solution and water
  4. dry with materialThe soluiton was dried (anhydrous magnesium sulfate)
  5. customevaporated
  6. customthe solid residue crystallized from ethyl acetate
  7. customto afford 1.4

出典と根拠

ORDレコード
ord-449562b410bc4fbd8e5e841defa7045c
出典データセット
uspto-grants-1984_05
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04446071

反応ノート

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