a Farnesol → 3,7,11-Trimethyl-1-dodecanol
反応式
[OH:1][CH2:2][CH:3]=[C:4]([CH2:6][CH2:7][CH:8]=[C:9]([CH2:11][CH2:12][CH:13]=[C:14]([CH3:16])[CH3:15])[CH3:10])[CH3:5]>C(O)C.[Pt]=O>[CH3:5][CH:4]([CH2:6][CH2:7][CH2:8][CH:9]([CH3:10])[CH2:11][CH2:12][CH2:13][CH:14]([CH3:16])[CH3:15])[CH2:3][CH2:2][OH:1]参加物
4
実験手順
Farnesol (200 g) was dissolved in ethanol (1000 ml), added with platinum oxide (1 g) and stirred for 24 hours at room temperature under hydrogen atmosphere. After the completion of the reaction, insoluble material was removed by filtration through a Celite layer and the filtrate was concentrated under reduced pressure to obtain 3,7,11-trimethyldodecanol (195 g).
後処理
- customAfter the completion of the reaction, insoluble material
- customwas removed by filtration through a Celite layer
- concentrationthe filtrate was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-d6aa1484224448e995eff7bbe4db6fd5
- 出典データセット
- uspto-grants-1993_09
- 特許番号
- US05245070
反応ノート
読み込み中…