Sodium Chloride → EDTA disodium salt

HRID 593330

反応式

HRID 593330 の反応式
[CH2:1]([N:12]([CH2:17][C:18]([OH:20])=[O:19])[CH2:13][C:14]([OH:16])=[O:15])[CH2:2][N:3]([CH2:8][C:9]([OH:11])=[O:10])[CH2:4][C:5]([OH:7])=[O:6].[Cl-].[Na+:22]>O>[CH2:2]([N:3]([CH2:8][C:9]([O-:11])=[O:10])[CH2:4][C:5]([OH:7])=[O:6])[CH2:1][N:12]([CH2:17][C:18]([O-:20])=[O:19])[CH2:13][C:14]([OH:16])=[O:15].[Na+:22].[Na+:22]

参加物

4

反応物 2

HCID 5234Sodium ChlorideHCID 6049Ethylenediaminetetraacetic Acid

生成物 1

HCID 8759EDTA disodium salt

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
65 °C

実験手順

Crude MTC product (MW 373.90, 10.0 g, ˜26.7 mmol) was fully dissolved in H2O (270 cm3). Ethylenediaminetetraacetic acid (EDTA) disodium salt dihydrate (MW 372.24, 1 g, 2.68 mmol, 0.1 equivalents) was added. The mixture was stirred at 65° C. for approximately 1 hour. The mixture was filtered by vacuum filtration. The filtrate was collected. Sodium chloride (NaCl, MW 57.96, 16 g, 0.276 mol, 10 equivalents) was added to the filtrate while stirring. The resulting precipitate was collected by vacuum filtration.

後処理

  1. filtrationThe mixture was filtered by vacuum filtration
  2. customThe filtrate was collected
  3. stirringwhile stirring
  4. filtrationThe resulting precipitate was collected by vacuum filtration

出典と根拠

ORDレコード
ord-24ff0427a43947f48c65db3449de5a0a
出典データセット
uspto-grants-2016_01
特許番号
US09242946B2

関連ノート

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