Methyl iodide → HCID 20370520、化合物

反応式

[CH3:1][N:2]([CH3:19])[C:3](=[O:18])[CH:4]([CH3:17])[N:5]1[CH:9]=[C:8]([CH3:10])[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1.[CH3:20]I.[CH2:22](I)[CH3:23]>>[CH3:19][N:2]([CH3:1])[C:3](=[O:18])[C:4]([CH3:20])([CH3:17])[N:5]1[CH:9]=[C:8]([CH2:10][CH2:22][CH3:23])[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1

参加物

反応物 3

HCID 6328Methyl iodide

HCID 6340Iodoethane

HCID 20370501N,N-dimethyl-2-(4-methyl-3-phenyl-1H-pyrazol-1-yl)propanamide

生成物 1

HCID 20370520HCID 20370520、化合物

実験手順

Following the procedure of Example 95, but substituting N,N,α-trimethyl-3-phenyl-4-propylpyrazole-1-acetamide for N,N,α,4-tetramethyl-3-phenypyrazole-1-acetamide and methyl iodide for ethyl iodide, there was obtained N,N,α,α-tetramethyl-3-phenyl-4-propylpyrazole-1-acetamide, m.p. 98.5°-101° C.

出典と根拠

ORDレコード: ord-2b94a09c5abd436f98c43ea802aa1b01
出典データセット: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04072498

反応ノート

読み込み中…

参加物