反応式
[Cl-].[NH4+].[Cl-].[Nd+3:4].[Cl-].[Cl-].[C:7](=[O:10])([O-:9])[O-:8].[Na+].[Na+]>[Co](Cl)Cl>[C:7](=[O:8])([O-:10])[O-:9].[Nd+3:4].[C:7](=[O:8])([O-:10])[O-:9].[C:7](=[O:8])([O-:10])[O-:9].[Nd+3:4]参加物
5
反応条件
- 温度
- 50 °C
実験手順
A solution of cobalt chloride having a gravity of 1.20 g/cm3 containing ammonium chloride was mixed while stirring with a solution of neodymium chloride and heated to 50° C. A stoichiometric equivalent quantity of sodium carbonate solution of 60° C. having a gravity of 1.05 g/cm3 was added to the mixed solution while stirring. The precipitates of cobalt carbonate and neodymium carbonate were obtained after reaction, filtrated in a vacuum filtrator to remove the mother liquid, washed by distilled water of 90° C. for 6 times, dried at 200° C., crushed and sieved by a 20 mesh sieve, reduced at 600° C. in hydrogen for 3 h, then crushed again and sieved by a 100 mesh sieve. The prepared cobalt powder contained 2.8% (wt.) neodymium.
後処理
- additionwas mixed
- additionwas added to the mixed solution
- customThe precipitates of cobalt carbonate
出典と根拠
- ORDレコード
- ord-155ed44d0c004f6b88a366ddb1f96444
- 出典データセット
- uspto-grants-1993_09
- 特許番号
- US05248328
関連ノート
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