Cyclohexylamine → 8-Methylnonanoic acid cyclohexylamine salt
反応式
[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10].[CH:13]1([NH2:19])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1>CCCCCCC>[CH:13]1([NH2:19])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1.[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10]参加物
4
実験手順
From the 8-methylnonanoic acid crude product obtained in Example 1, 8.00 g was dissolved in heptane (30 ml). Cyclohexylamine (6.91 ml, 60.4 mmol) was slowly added dropwise at 0° C. (ice bath), and the mixture was stirred at room temperature for 20 minutes. The reaction mixture was filtered to give 8-methylnonanoic acid cyclohexylamine salt (15.7 g).
後処理
- filtrationThe reaction mixture was filtered
出典と根拠
- ORDレコード
- ord-f0e91b54879e4f9caeab73e5e708080f
- 出典データセット
- uspto-grants-2010_04
- 特許番号
- US07700331B2
反応ノート
読み込み中…