Cyclohexylamine → 8-Methylnonanoic acid cyclohexylamine salt

HRID 643199

反応式

HRID 643199 の反応式
[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10].[CH:13]1([NH2:19])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1>CCCCCCC>[CH:13]1([NH2:19])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1.[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10]

参加物

4

反応物 2

HCID 7965CyclohexylamineHCID 1114708-Methylnonanoic acid

生成物 1

HCID 686053248-Methylnonanoic acid cyclohexylamine salt

試薬・触媒・溶媒 1

HCID 8900Heptane溶媒

実験手順

From the 8-methylnonanoic acid crude product obtained in Example 1, 8.00 g was dissolved in heptane (30 ml). Cyclohexylamine (6.91 ml, 60.4 mmol) was slowly added dropwise at 0° C. (ice bath), and the mixture was stirred at room temperature for 20 minutes. The reaction mixture was filtered to give 8-methylnonanoic acid cyclohexylamine salt (15.7 g).

後処理

  1. filtrationThe reaction mixture was filtered

出典と根拠

ORDレコード
ord-f0e91b54879e4f9caeab73e5e708080f
出典データセット
uspto-grants-2010_04
特許番号
US07700331B2

関連ノート

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