Hydrochloric Acid → HCID 20142835、化合物
反応式
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][C:11]([OH:13])=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1N=CN(C(N2C=NC=C2)=O)C=1.[CH2:26]([O:28][C:29](=[O:32])[CH2:30][NH2:31])[CH3:27].Cl.N(CC)(CC)CC>C1COCC1>[CH2:26]([O:28][C:29](=[O:32])[CH2:30][NH:31][C:11](=[O:13])[CH2:10][CH2:9][CH2:8][CH2:7][C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)[CH3:27]参加物
7
実験手順
5-Phenylvaleric acid (2.67 g, 15 mmol) in distilled THF was reacted with CDI (15 mmol) followed by glycine ethyl ester.HCl (15 mmol) and (C2H5)3N (15 mmol) as described in Example 35 Part A. The crude material (3.25 g, 82%) was used without purification.
後処理
- customThe crude material (3.25 g, 82%) was used without purification
出典と根拠
- ORDレコード
- ord-49b1f8802f494b2cbee06953f26009d3
- 出典データセット
- uspto-grants-1988_04
- 特許番号
- US04735962
反応ノート
読み込み中…