Heptane → Toluene heptane

HRID 653847

反応式

HRID 653847 の反応式
BrC1C=C(Br)C=CC=1OP(OC1C=CC(Br)=CC=1Br)(OC1C=CC(Br)=CC=1Br)=O.[CH3:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36].BrC1C=C(Br)C=CC=1O>C1(C)C=CC=CC=1>[CH3:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36].[C:31]1([CH3:30])[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1

参加物

5

反応物 3

HCID 8900HeptaneHCID 120052,4-DibromophenolHCID 14670658Phenol, 2,4-dibromo-, phosphate (3:1)

生成物 1

HCID 22263336Toluene heptane

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

Two hundred and eighty-four grams of crude tris-(2,4-dibromophenyl)phosphate were mixed with 808 grams of a solution of 85% n-heptane and 15% toluene as above. The liquid portion weighed 733 grams and contained 0.047% 2,4-dibromophenol, 1.45% ester product and 0.06% chloridates.

出典と根拠

ORDレコード
ord-555e4b438369405a8d9ce68fee2899ca
出典データセット
uspto-grants-1992_07
特許番号
US05128496

関連ノート

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