5-(1-Naphthyl)-4-pentyn-1-ol → 5-(Naphth-1-yl)pentanol

HRID 654954

反応式

HRID 654954 の反応式
[C:1]1([C:11]#[C:12][CH2:13][CH2:14][CH2:15][OH:16])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1>C(OCC)C.[Pd]>[C:1]1([CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][OH:16])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1

参加物

4

反応物 1

HCID 199555575-(1-Naphthyl)-4-pentyn-1-ol

生成物 1

HCID 103532005-(Naphth-1-yl)pentanol

試薬・触媒・溶媒 2

HCID 23938Palladium触媒HCID 3283Diethyl Ether溶媒

実験手順

A mixture of 5-(1-naphthyl)-4-pentyn-1-ol (500 ng, 2.37 mmol) and 5% palladium on barium sulfate (5 mg) in ethyl ether (30 ml) was stirred at room temperature under a hydrogen atmosphere for two days. Solvent removal, after filtration through celite, gave the title compound as a yellow oil.

後処理

  1. customSolvent removal
  2. filtrationafter filtration through celite

出典と根拠

ORDレコード
ord-fc1489072aa34dfd8d39a00b9d7dfcbb
出典データセット
uspto-grants-1992_07
特許番号
US05134128

関連ノート

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