Diethylmethylamine → Methanesulfonic acid, 1,1,1-trifluoro-, compd. with N-ethyl-N-methylethanamine (1:1)

HRID 655087

反応式

HRID 655087 の反応式
[CH2:1]([N:3]([CH2:5][CH3:6])[CH3:4])[CH3:2].[F:7][C:8]([F:14])([F:13])[S:9]([OH:12])(=[O:11])=[O:10]>>[F:7][C:8]([F:14])([F:13])[S:9]([O-:12])(=[O:11])=[O:10].[CH2:1]([NH+:3]([CH2:5][CH3:6])[CH3:4])[CH3:2]

参加物

3

反応物 2

HCID 12022Diethylmethylamine2 回HCID 62406Trifluoromethanesulfonic acid2 回

生成物 1

HCID 86620365Methanesulfonic acid, 1,1,1-trifluoro-, compd. with N-ethyl-N-methylethanamine (1:1)

実験手順

Equimolar amounts of diethylmethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed diethylmethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

後処理

  1. temperaturewhile being cooled by liquid nitrogen
  2. customthus obtaining a target ionic conductor

出典と根拠

ORDレコード
ord-9f5289c08f2941199dbef871e4dcb7eb
出典データセット
uspto-grants-2011_12
特許番号
US08071253B2

関連ノート

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