Hexamethylenetetramine → Molybdenum hexamethylenetetramine

HRID 65826

反応式

HRID 65826 の反応式
[CH2:1]1[N:6]2[CH2:7][N:8]3[CH2:10][N:4]([CH2:5]2)[CH2:3][N:2]1[CH2:9]3.O[Mo:12](O)(=O)=O.[NH4+].[NH4+].[O-][Mo]([O-])(=O)=O>O>[Mo:12].[CH2:1]1[N:6]2[CH2:7][N:8]3[CH2:10][N:4]([CH2:5]2)[CH2:3][N:2]1[CH2:9]3

参加物

5

反応物 3

HCID 4101HexamethylenetetramineHCID 61578Diammonium molybdateHCID 82208Molybdic acid

生成物 1

HCID 131710930Molybdenum hexamethylenetetramine

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

Hexamethylenetetramine molybdate having a 2/1 molybdenum/hexamethylenetetramine molar ratio was prepared as follows. 10 grams of hexamethylenetetramine was dissolved in 100 ml water heated near reflux temperature. 24.01 grams of commercial, so-called "molybdic acid" (actually at least one ammonium molybdate) was dissolved in 169 ml water heated to reflux temperature. The first solution was added to the second solution.

後処理

  1. temperatureheated
  2. temperaturenear reflux temperature
  3. temperatureheated
  4. temperatureto reflux temperature
  5. additionThe first solution was added to the second solution

出典と根拠

ORDレコード
ord-242010b0e43b497ba711f280db016fe8
出典データセット
uspto-grants-1978_12
特許番号
US04129540

関連ノート

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