Water → HCID 15729558、化合物
反応式
F[C:2]1[N:7]=[C:6]([S:8](Cl)(=[O:10])=[O:9])[CH:5]=[CH:4][CH:3]=1.Cl.[O:13](N)[CH3:14].C([N:18]([CH2:21]C)CC)C.[OH2:23]>C(Cl)(Cl)Cl>[CH3:14][O:13][N:18]([CH3:21])[S:8]([C:6]1[CH:5]=[CH:4][CH:3]=[C:2]([O:23][S:8]([CH3:6])(=[O:10])=[O:9])[N:7]=1)(=[O:10])=[O:9]参加物
6
実験手順
A solution of 6-fluoropyridine-2-sulphonylchloride (1.96 g) and methoxylamine hydrochloride (1.96 g) in chloroform (40 cm3) was cooled to -78° C. under an atmosphere of nitrogen and a solution of triethylamine (2.03 g) in chloroform (10 cm3) was added with stirring. The reaction mixture was added to water and the product extracted into chloroform. The combined organic layers were dried over magnesium sulphate, filtered and evaporated to give the title product.
後処理
- extractionthe product extracted into chloroform
- dry with materialThe combined organic layers were dried over magnesium sulphate
- filtrationfiltered
- customevaporated
出典と根拠
- ORDレコード
- ord-ac0c0438638f4a129843754e9c188ddc
- 出典データセット
- uspto-grants-1991_01
- 特許番号
- US04987141
反応ノート
読み込み中…