L-Phenylalanine → HCID 68631493、化合物

HRID 72100

反応式

HRID 72100 の反応式
[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[C:13]([O:18]C(=O)CCC)(=O)[CH2:14][CH2:15][CH3:16]>>[C:13]([NH2:1])(=[O:18])[CH2:14][CH2:15][CH3:16].[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

参加物

3

反応物 2

HCID 6140L-PhenylalanineHCID 7798Butyric anhydride

生成物 1

HCID 68631493HCID 68631493、化合物

反応条件

温度
100 °C

実験手順

5 g of phenylalanine was added to 20 mL of butyric anhydride and the resulting mixture heated to about 100° C. for about 3 h. Excess butyric anhydride was then removed under reduced pressure to provide a solid residue that was recrystallized from ethanol to provide phenylalanine butyramide.

後処理

  1. customExcess butyric anhydride was then removed under reduced pressure
  2. customto provide a solid residue that
  3. customwas recrystallized from ethanol

出典と根拠

ORDレコード
ord-3e84eb0ed57b475cbbdee34bf3c5aaeb
出典データセット
uspto-grants-2014_09
特許番号
US08828960B2

関連ノート

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