Hydrochloric Acid → HCID 19427131、化合物

HRID 741788

反応式

HRID 741788 の反応式
[CH2:1]([Si:9](Cl)(Cl)Cl)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH3:13][O:14][CH2:15][CH2:16][O:17][CH2:18][CH2:19][OH:20].Cl>CCCCCCC>[CH2:1]([Si:9]([O:20][CH2:19][CH2:18][O:17][CH2:16][CH2:15][O:14][CH3:13])([O:20][CH2:19][CH2:18][O:17][CH2:16][CH2:15][O:14][CH3:13])[O:20][CH2:19][CH2:18][O:17][CH2:16][CH2:15][O:14][CH3:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 8134Diethylene Glycol Monomethyl EtherHCID 21354Octyltrichlorosilane

生成物 1

HCID 19427131HCID 19427131、化合物

試薬・触媒・溶媒 1

HCID 8900Heptane溶媒

反応条件

温度
80 °C

実験手順

To a dry flask fitted with an agitator, thermometer, additional funnel and reflux condenser was charged 222.8 g (0.90 mole) of octyltrichlorosilane and 225 g of heptane. The mixture was blanketed with nitrogen, heated to 80° C. and 333.7 g (2.78 mole) of 2-(2-methoxyethoxy)ethanol was added slowly over a 2 hour period. Hydrogen chloride was evolved from the mixture. After the addition was complete heating of the reaction was continued for 24 hours at 80° C. Then the solvent and all volatile components of the mixture were removed under vacuum, producing 451 g of the clear, colorless liquid product.

後処理

  1. customTo a dry flask fitted with an agitator
  2. temperaturethermometer, additional funnel and reflux condenser
  3. additionAfter the addition
  4. temperaturewas complete heating of the reaction
  5. customThen the solvent and all volatile components of the mixture were removed under vacuum
  6. customproducing 451 g of the clear, colorless liquid product

出典と根拠

ORDレコード
ord-52c37a1263d54e1fabd252f7eb585341
出典データセット
uspto-grants-1996_09
特許番号
US05552476

関連ノート

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