Hydrochloric Acid → Benzoic acid, 2-(aminosulfonyl)-, methyl ester
反応式
Cl.[S:2]1([C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:6](=[O:7])[NH:5]1)(=[O:4])=[O:3].[CH3:14][OH:15]>>[CH3:14][O:15][C:6](=[O:7])[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=1[S:2](=[O:4])(=[O:3])[NH2:5]参加物
4
実験手順
An HCl stream is led under cooling into a suspension of 143.3 g (0.78 mol) in 600 ml absolute methanol until saturation. Subsequently the solution is refluxed yet two hours until the saccharine has gone completely into solution and the reaction has terminated.
後処理
- customthe reaction has terminated
出典と根拠
- ORDレコード
- ord-7682b66929384626b8eedbdba4fb52da
- 出典データセット
- uspto-grants-1986_07
- 特許番号
- US04601746
反応ノート
読み込み中…