反応式
[CH3:1][C:2]([CH3:7])([CH3:6])[CH2:3][CH:4]=O.[O:8]1[CH2:13][CH2:12][CH:11]([NH2:14])[CH2:10][CH2:9]1.[S-:15][C:16]#[N:17].[K+].II>>[C:2]([C:3]1[S:15][C:16](=[NH:17])[N:14]([CH:11]2[CH2:12][CH2:13][O:8][CH2:9][CH2:10]2)[CH:4]=1)([CH3:7])([CH3:6])[CH3:1]参加物
5
実験手順
Commercially available 3,3-dimethylbutanal (Aldrich), tetrahydro-2H-pyran-4-amine (Matrix), potassium thiocyanate (Aldrich) and iodine (EMD chemicals) were processed using the method described in Example 315A to afford the title compound. MS (ESI+) m/z 241 (M+H)+.
出典と根拠
- ORDレコード
- ord-ef468d2d183b4ba09924b14ea3fde380
- 出典データセット
- uspto-grants-2014_09
- 特許番号
- US08841334B2
関連ノート
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