Hydroquinone → Butyl hydroxy[(2-methylacryloyl)amino]acetate

HRID 845875ノート

反応式

HRID 845875 の反応式
C(O[CH:6]([OH:14])[C:7]([O:9][CH2:10][CH2:11][CH2:12][CH3:13])=[O:8])CCC.[C:15]([NH2:20])(=[O:19])[C:16]([CH3:18])=[CH2:17].COC.C1(C=CC(O)=CC=1)O.C(OC(NC(=O)C=CC)C(OCCCC)=O)CCC>>[C:15]([NH:20][CH:6]([OH:14])[C:7]([O:9][CH2:10][CH2:11][CH2:12][CH3:13])=[O:8])(=[O:19])[C:16]([CH3:18])=[CH2:17]

参加物

6

反応物 5

HCID 785HydroquinoneHCID 6595MethacrylamideHCID 8254Dimethyl EtherHCID 109478Acetic acid, 2-butoxy-2-hydroxy-, butyl esterHCID 131715646HCID 131715646、化合物

生成物 1

HCID 18954900Butyl hydroxy[(2-methylacryloyl)amino]acetate

実験手順

The procedure of example VI was again followed using the following change: butyl glyoxylate butyl hemiacetal 273 parts; methacrylamide 110 parts; methyl ether of hydroquinone 0.27 parts. The reaction was run at 70° to 75° C. for 1.5 hours. The material was not isolated, instead it was used directly to make butyl methylacrylamidoglycolate butyl ether.

後処理

  1. customThe material was not isolated

出典と根拠

ORDレコード
ord-ea255366bcdf40f4bbcd562039dae57d
出典データセット
uspto-grants-1988_07
特許番号
US04760168

反応ノート

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