反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([NH:11][C:12]2[CH:17]=[CH:16][C:15]([S:18][CH3:19])=[CH:14][CH:13]=2)C#N)=[CH:4][CH:3]=1.C(C=C)=O>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[N:11][C:12]2[CH:17]=[CH:16][C:15]([S:18][CH3:19])=[CH:14][CH:13]=2)=[CH:4][CH:3]=1参加物
3
実験手順
Following a procedure similar to that described in Example 21(iii), but using α-(4-chlorophenyl)-α-(4-methylthioanilino)acetonitrile [prepared as described in step (ii) above] and acrolein as starting materials, the title compound was obtained as an orange-colored powder (yield 32%), melting at 203-205° C.
出典と根拠
- ORDレコード
- ord-e8566af10da04d4cb67722f52d006b8e
- 出典データセット
- uspto-grants-2006_12
- 特許番号
- USRE039420E1
関連ノート
読み込み中…