2-Propenoic acid, 3-phenyl- → 1-Indanone, 3-phenyl-

HRID 863614

反応式

HRID 863614 の反応式
[Cl-].[Al+3].[Cl-].[Cl-].[C:5]([OH:15])(=O)[CH:6]=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>C1C=CC=CC=1>[C:8]1([CH:7]2[C:8]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[C:5](=[O:15])[CH2:6]2)[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

参加物

4

反応物 2

HCID 87842-Propenoic acid, 3-phenyl-HCID 6451240Aluminum(III) Chloride

生成物 1

HCID 981461-Indanone, 3-phenyl-収率 85.4%

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

To 25.0 g of aluminum chloride, 8.5 g of cinnamic acid and 37.5 ml of benzene were added and the mixture was reacted under reflux for 5 hours. The reaction solution was processed by a usual method to obtain 5.1 g of 3-phenyl-1-indanone.

後処理

  1. customthe mixture was reacted
  2. temperatureunder reflux for 5 hours

出典と根拠

ORDレコード
ord-a49f611610274bb892e899afe57aaf15
出典データセット
uspto-grants-1998_02
特許番号
US05721288

関連ノート

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