Sodium Hydroxide → Leucinamide

HRID 864277

反応式

HRID 864277 の反応式
[NH2:1][C@H:2]([C:7]([NH2:9])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5].Cl.[OH-].[Na+]>CC(N(C)C)=O.O>[NH2:1][C@H:2]([C:7]([NH2:9])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5]

参加物

5

反応物 2

HCID 14798Sodium HydroxideHCID 2733199Leucinamide hydrochloride

生成物 1

HCID 69640Leucinamide

試薬・触媒・溶媒 2

HCID 962Water溶媒HCID 31374Dimethylacetamide溶媒2 回

実験手順

1.25M solution of Leu-NH2 in DMAC was prepared by dissolving Leu-NH2.HCl (1.33 g, 7.98 mmol) in 5.0 mL of water, titrating to pH 8.0 with 1M NaOH, lyophilizing, and taking up the residue in 6.4 ml of DMAC. The NaCl precipitate was removed by filtering through a fine glass frit to give a clear solution of pH 9.25.

後処理

  1. customThe NaCl precipitate was removed
  2. filtrationby filtering through a fine glass frit
  3. customto give a clear solution of pH 9.25

出典と根拠

ORDレコード
ord-b5d127ef1e6044608b68a102b37d5fbf
出典データセット
uspto-grants-1996_10
特許番号
US05563044

関連ノート

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