反応式
C([O-])(=O)CCCC[CH2:6][C:7](C)([CH3:9])[CH3:8].[CH2:13]([C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([CH2:21][CH3:22])[C:16]=1[N:23]1[C:27](=[O:28])[CH:26]=[CH:25][C:24]1=[O:29])[CH3:14].C=C(C)C>C1(C)C=CC=CC=1>[CH2:13]([C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([CH2:21][CH3:22])[C:16]=1[N:23]1[C:24](=[O:29])[CH:25]=[CH:26][C:27]1=[O:28])[CH3:14].[CH2:6]=[C:7]([CH3:9])[CH3:8]参加物
5
実験手順
In a one-liter autoclave were charged 400 ml of toluene as a polymerization solvent, 0.001 moles of perbutyl neodecanoate as a polymerization initiator, 0.42 moles of N-(2,6-diethylphenyl)maleimide, and 4.05 moles of isobutene, and the mixture was subjected to polymerization reaction under a polymerization condition at a polymerization temperature of 60° C. for a polymerization time of 5 hours, to obtain N-(2,6-diethylphenyl)maleimide-isobutene alternating copolymer. The thus obtained N-(2,6-diethylphenyl)maleimide-isobutene alternating copolymer had a weight average molecular weight (Mw) (as reduced into standard polystyrene) of 170,000 and an Mw/Mn of 2.6.
後処理
- customthe mixture was subjected to polymerization reaction under a polymerization condition at a polymerization temperature of 60° C. for a polymerization time of 5 hours
出典と根拠
- ORDレコード
- ord-83c839dd95dc4cd6a3de8857d7f8c45d
- 出典データセット
- uspto-grants-2006_02
- 特許番号
- US07001967B2
関連ノート
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