Isopropylamine → N-Isopropylmethacrylamide

反応式

[C:1]([O:6]C)(=O)[C:2]([CH3:4])=[CH2:3].[CH:8]([NH2:11])([CH3:10])[CH3:9]>>[CH:8]([NH:11][C:1](=[O:6])[C:2]([CH3:4])=[CH2:3])([CH3:10])[CH3:9]

参加物

反応物 2

HCID 6363Isopropylamine

HCID 6658Methyl Methacrylate

生成物 1

HCID 83698N-Isopropylmethacrylamide収率 32%

実験手順

200 g of methyl methacrylate and 142 g of isopropylamine were heated at 190° C. for 21/2 hours in a 0.5-liter stirred autoclave (pmax =15 atmospheres). N-isopropyl-methacrylic acid amide was formed in this way in a 32% yield.

出典と根拠

ORDレコード: ord-8bd2f0698eaf4139be03c1b377c0d6eb
出典データセット: uspto-grants-1980_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04228102

反応ノート

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