Water → HCID 86752776、化合物

HRID 963913

反応式

HRID 963913 の反応式
C1C=C([N+]([O-])=O)N(CCO)C=1C(N)=O.O.[C:16]([CH2:19][C:20](=[O:22])[CH3:21])(=[O:18])[CH3:17].CCCCOC(C1C(C(OCC2C=CC=CC=2)=O)=CC=CC=1)=O>CC(C)=O>[C:16]([CH2:19][C:20](=[O:22])[CH3:21])(=[O:18])[CH3:17].[CH3:17][C:16]([CH3:19])=[O:18]

参加物

7

反応物 5

HCID 962Water2 回HCID 2347Butyl Benzyl PhthalateHCID 31261AcetylacetoneHCID 1606551-(2-Hydroxyethyl)-5-nitro-1H-pyrrole-2-carboxamideHCID 178435178HCID 178435178、化合物

生成物 1

HCID 86752776HCID 86752776、化合物

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

On the first day, 1.31 grams of dispersant, NP-10 (Union Carbide), 1.6 grams of high-resistivity water (very pure water prepared in-house for semiconductor work) and 15 grams of solvent mixture (made from 172 ml acetone and 28 ml acetylacetone) were added and mixed well in a 250 ml polypropylene bottle. Then, 13.0 grams of borosilicate glass powder and 8.75 grams of quartz were added into the mixture and ball milled overnight using 10 mm diameter ZrO2 balls. On the second day, 0.2 gram of binder, Butvar B79 (Monsanto) was added into the mixture and ball milled for one hour. Then 2.41 grams of B79, 2.61 grams of plasticizer, Santicizer 160 (butyl phthalate from Monsanto) were added into the bottle and milled for about 3 hours to obtain a creamy, smooth mixture known as a slip or slurry. The slip was cast on a carrier of Fujimori Mylar™ using a 6 inch wide doctor blade having a 16 mil gap at 14 ft/min at room temperature.

後処理

  1. additionwere added
  2. custommilled overnight
  3. additionOn the second day, 0.2 gram of binder, Butvar B79 (Monsanto) was added into the mixture and ball
  4. custommilled for one hour
  5. custommilled for about 3 hours
  6. customto obtain a creamy, smooth mixture
  7. customat room temperature

出典と根拠

ORDレコード
ord-fc9f3bca285e4359abfa9a73511196ee
出典データセット
uspto-grants-1998_06
特許番号
US05766528

関連ノート

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