Triethylamine → HCID 21922276、化合物

HRID 979725

反応式

HRID 979725 の反応式
C(N(CC)CC)C.[CH2:8]([CH:10]([CH2:14][CH2:15][CH2:16][CH3:17])[C:11]([OH:13])=[O:12])[CH3:9].[Cl-].[Cr+2:19].[Cl-]>CCCCCCC>[CH2:8]([CH:10]([CH2:14][CH2:15][CH2:16][CH3:17])[C:11]([O-:13])=[O:12])[CH3:9].[CH2:8]([CH:10]([CH2:14][CH2:15][CH2:16][CH3:17])[C:11]([O-:13])=[O:12])[CH3:9].[Cr+2:19]

参加物

5

反応物 3

HCID 8471TriethylamineHCID 86972-Ethylhexanoic AcidHCID 10197677chromium(II) dichloride

生成物 1

HCID 21922276HCID 21922276、化合物

試薬・触媒・溶媒 1

HCID 8900Heptane溶媒2 回

実験手順

Chromium (II) bis(2-ethylhexanoate) is prepared by the addition of an equimolar mixture of triethylamine and 2-ethylhexanoic acid in heptane to a suspension of 0.5 mole anhydrous chromium (II) chloride in heptane. A slow reaction results in the formation of a deep purple solution and the precipitation of triethylammonium hydrochloride. The product is isolated as a purple oil after removal of the precipitate by filtration and the volatiles under vacuum.

後処理

  1. customA slow reaction
  2. customresults in the formation of a deep purple solution
  3. customthe precipitation of triethylammonium hydrochloride
  4. customThe product is isolated as a purple oil
  5. customafter removal of the precipitate
  6. filtrationby filtration

出典と根拠

ORDレコード
ord-d2533a5280b044d7bc482e2666c224f8
出典データセット
uspto-grants-1987_05
特許番号
US04668838

関連ノート

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