Isopropanol → Yttrium(iii) isopropoxide
反応式
[Y:1].[CH:2]([OH:5])([CH3:4])[CH3:3]>[Cl-].[Cl-].[Zn+2].[Zn]>[CH3:3][CH:2]([CH3:4])[O-:5].[Y+3:1].[CH3:3][CH:2]([CH3:4])[O-:5].[CH3:3][CH:2]([CH3:4])[O-:5]参加物
5
実験手順
The same procedure described in Example 3 was utilized except that ZnCl2 was substituted for zinc metal but was not milled with the yttrium. The milled yttrium, without zinc metal or zinc chloride, was reacted with a solution of isopropanol (500 cc) and 3 grams of ZnCl2 over a 24 hour period. Work-up of the reaction mixture yielded 41.6 grams (a 70% yield) of yttrium isopropoxide.
出典と根拠
- ORDレコード
- ord-dac3355981c3471781afc681e54aba5f
- 出典データセット
- uspto-grants-1991_02
- 特許番号
- US04996300
反応ノート
読み込み中…