2-Aminopyrimidine → HCID 9795705、化合物
反応式
[NH2:1][C:2]1[N:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[CH2:8]([N+:12]#[C-:13])[CH2:9][CH2:10][CH3:11].[CH3:14][C:15]1[CH:22]=[CH:21][CH:20]=[CH:19][C:16]=1[CH:17]=O>Cl(O)(=O)(=O)=O>[CH2:8]([NH:12][C:13]1[N:3]2[CH:4]=[CH:5][CH:6]=[N:7][C:2]2=[N:1][C:14]=1[C:15]1[CH:22]=[CH:21][CH:20]=[CH:19][C:16]=1[CH3:17])[CH2:9][CH2:10][CH3:11]参加物
5
実験手順
Compound (14) was prepared in accordance with the general instructions from 1.0 ml 2-aminopyrimidine solution (0.1 M, MC), 0.575 ml n-butylisonitrile solution (0.2 M, MC), 0.500 ml 2-methylbenzaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%).
出典と根拠
- ORDレコード
- ord-fc857b1fb3ab482285400342098adf03
- 出典データセット
- uspto-grants-2003_10
- 特許番号
- US06638933B2
反応ノート
読み込み中…