Methanol → 2,6-Di-tert-butyl-4-(methoxymethyl)phenol

HRID 1004437

반응식

HRID 1004437 반응식
[OH:1][CH2:2][C:3]1[CH:8]=[C:7]([C:9]([CH3:12])([CH3:11])[CH3:10])[C:6]([OH:13])=[C:5]([C:14]([CH3:17])([CH3:16])[CH3:15])[CH:4]=1.[CH3:18]O>Cl>[CH3:18][O:1][CH2:2][C:3]1[CH:4]=[C:5]([C:14]([CH3:17])([CH3:16])[CH3:15])[C:6]([OH:13])=[C:7]([C:9]([CH3:10])([CH3:11])[CH3:12])[CH:8]=1

참가 물질

4

반응물 2

HCID 887MethanolHCID 6929Butylated hydroxymethylphenol

생성물 1

HCID 69112,6-Di-tert-butyl-4-(methoxymethyl)phenol수율 94%

시약·촉매·용매 1

HCID 313Hydrochloric Acid촉매

실험 절차

A solution of 4-hydroxymethyl-2,6-di-t-butylphenol (0.5 g) in methanol (10 mL) containing 1 drop of concentrated hydrochloric acid was stirred at ambient temperature for 1 hour. Evaporation of the solvent gave the title compound, 0.5 g, 94% yield as a white crystalline solid.

후처리

  1. customEvaporation of the solvent

출처 및 근거

ORD 기록
ord-113efb57cef44a829e4e591636f562cf
출처 데이터셋
uspto-grants-2000_04
특허 번호
US06048995

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