반응식
[CH2:1]([O:8][C:9]1[CH:10]=[C:11]([CH2:18][C:19]#[N:20])[CH:12]=[CH:13][C:14]=1[N+:15]([O-:17])=[O:16])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.B#B.[ClH:23]>>[ClH:23].[CH2:1]([O:8][C:9]1[CH:10]=[C:11]([CH2:18][CH2:19][NH2:20])[CH:12]=[CH:13][C:14]=1[N+:15]([O-:17])=[O:16])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1참가 물질
4
실험 절차
2.7 g of (3-benzyloxy-4-nitrophenyl)acetonitrile is reduced with diborane, as described in the preparation of 2-benzyloxy-5-(2-dipropylamino)aniline, and converted into the hydrochloride, thus obtaining 3.2 g of 2-(3-benzyloxy-4-nitrophenyl)ethylamine, hydrochloride.
출처 및 근거
- ORD 기록
- ord-7106c923e7aa46ec8d4205d4e24c899c
- 출처 데이터셋
- uspto-grants-1990_09
- 특허 번호
- US04958026
연결된 노트
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