Triethylamine → 1,3-Bis(trichlorosilyl)propane

HRID 1068532

반응식

HRID 1068532 반응식
C(N(CC)CC)C.Cl[CH2:9][CH2:10][CH2:11]Cl.[Cl:13][SiH:14]([Cl:16])[Cl:15]>>[Cl:13][Si:14]([Cl:16])([Cl:15])[CH2:9][CH2:10][CH2:11][Si:14]([Cl:16])([Cl:15])[Cl:13]

참가 물질

4

반응물 3

HCID 8471TriethylamineHCID 88811,3-DichloropropaneHCID 24811Trichlorosilane

생성물 1

HCID 112438561,3-Bis(trichlorosilyl)propane수율 9%

실험 절차

In the same apparatus and procedure as Example 1 above, 0.048 g (0.47 mmol) of triethylamine, 0.6 g (4.7 mmol) of 1,3-dichloropropane, and 3.18 g (23.5 mmol) of trichlorosilane were reacted at 200° C. for 15 hrs. The resulting mixture was distilled to give 0.13 g of 1,3-bis(trichlorosilyl)propane (yield; 9%).

후처리

  1. distillationThe resulting mixture was distilled

출처 및 근거

ORD 기록
ord-557893ce53c2404b9451f329735f3300
출처 데이터셋
uspto-grants-2001_06
특허 번호
US06251057B1

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