Hydrochloric Acid → HCID 13061754, 화합물

HRID 1075298노트

반응식

HRID 1075298 반응식
[CH:1]([N:4]([C:9]1[CH:16]=[C:15]([CH3:17])[CH:14]=[CH:13][C:10]=1[C:11]#[N:12])[C:5](OC)=[O:6])([CH3:3])[CH3:2].[OH:18]O.Cl>C(O)C.[OH-].[Na+]>[CH:1]([N:4]1[C:9]2[C:10](=[CH:13][CH:14]=[C:15]([CH3:17])[CH:16]=2)[C:11](=[O:18])[NH:12][C:5]1=[O:6])([CH3:3])[CH3:2]

참가 물질

6

반응물 3

HCID 313Hydrochloric AcidHCID 784Hydrogen PeroxideHCID 13061753HCID 13061753, 화합물

생성물 1

HCID 13061754HCID 13061754, 화합물

시약·촉매·용매 2

HCID 702Ethanol용매HCID 14798Sodium Hydroxide용매

실험 절차

To a suspension of 300 g 2-(N-isopropyl-N-carbomethoxyamino)-4-methyl-benzonitrile in 750 ml of ethanol and 234 ml 10N sodium hydroxide are added dropwise over 80 minutes 576 g of a 40% solution of hydrogen peroxide. The resulting clear solution is acidified with 195 ml of concentrated hydrochloric acid, whereupon the title compound precipitates, m.p. 250°-251°.

출처 및 근거

ORD 기록
ord-78ff9319128b4824b004d6edbe2fba76
출처 데이터셋
uspto-grants-1983_07
특허 번호
US04395550

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