Water → N-methyl-2H-3-isoquinolone

HRID 1075819

반응식

HRID 1075819 반응식
S(O)(O)(=O)=O.[CH3:6][N:7]1[C:16](=[O:17])[CH:15]=[C:14]2[C:9]([CH:10]=[CH:11][CH:12]=[CH:13]2)=[CH:8]1.O.C(=O)(O)[O-].[Na+]>C(Cl)(Cl)Cl>[CH3:6][N:7]1[C:16](=[O:17])[CH:15]=[C:14]2[C:9]([CH:10]=[CH:11][CH:12]=[CH:13]2)=[CH:8]1

참가 물질

5

반응물 3

HCID 962WaterHCID 516892Sodium BicarbonateHCID 21541268N-methyl-2H-3-isoquinolone sulfate

생성물 1

HCID 12435498N-methyl-2H-3-isoquinolone

시약·촉매·용매 1

HCID 6212Chloroform용매2회

실험 절차

70 g. N-methyl-2H-3-isoquinolone sulfate are dissolved, under an atmosphere of nitrogen, in 900 ml. water. 75 g. sodium bicarbonate are added and the mixture is stirred with 500 ml. chloroform. By decantation, there is obtained a chloroform solution of N-methyl-2H-3-isoquinolone, which can be dried over anhydrous sodium sulfate and employed as such or concentrated for a further reaction.

출처 및 근거

ORD 기록
ord-c078a18486cf4a12876c27b719da7b99
출처 데이터셋
uspto-grants-1976_05
특허 번호
US03954771

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