Oxalic Acid → HCID 178526029, 화합물

HRID 1077071

반응식

HRID 1077071 반응식
[O-2].[O-2].[O-2].[O-2].[O-2].[V+5:6].[V+5].[C:8]([OH:13])(=[O:12])[C:9]([OH:11])=[O:10]>[O-2].[O-2].[O-2].[K+].[Nb+5].O>[C:8]([O-:13])(=[O:12])[C:9]([O-:11])=[O:10].[V+5:6].[C:8]([O-:13])(=[O:12])[C:9]([O-:11])=[O:10].[C:8]([O-:13])(=[O:12])[C:9]([O-:11])=[O:10].[C:8]([O-:13])(=[O:12])[C:9]([O-:11])=[O:10].[C:8]([O-:13])(=[O:12])[C:9]([O-:11])=[O:10].[V+5:6]

참가 물질

5

반응물 2

HCID 971Oxalic AcidHCID 178419084HCID 178419084, 화합물

생성물 1

HCID 178526029HCID 178526029, 화합물

시약·촉매·용매 2

HCID 160967Niobium potassium oxide촉매HCID 962Water용매

반응 조건

온도
1300 °C

실험 절차

Granulated alumina (8 - 16 mesh) is heated at 1300°C. for 4 hours. Potassium niobate (4K2O.3Nb2O5.16H2O) and vanadium pentoxide are suspended in 5 parts of water, heated to 80°C., and oxalic acid is added slowly to obtain a blue-colored vanadium oxalate solution. Sodium carbonate is added and the alumina is also placed in the solution. The mixture is dried over a water bath with agitation. While air is pumped in, it is indurated in a furnace at 400°C. for 16 hours to obtain the catalyst ready for use after cooling.

후처리

  1. temperatureheated to 80°C.

출처 및 근거

ORD 기록
ord-a044738a2e224cfe80529a948e354241
출처 데이터셋
uspto-grants-1976_05
특허 번호
US03959336

연결된 노트

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