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2-Aminopropanol → 4-Methyl-2-undecyl-2-oxazoline

HRID 1086421
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HRID 1086421 반응식
[CH2:1]([C:12]#[N:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[CH3:14][CH:15](N)[CH2:16][OH:17]>C(O)CCC.O.O.C([O-])(=O)C.[Cd+2].C([O-])(=O)C>[CH3:14][CH:15]1[CH2:16][O:17][C:12]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])=[N:13]1
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참가 물질

5

반응물 2

HCID 51262-AminopropanolHCID 17092Dodecanenitrile

생성물 1

HCID 146517914-Methyl-2-undecyl-2-oxazoline수율 92%

시약·촉매·용매 2

HCID 6537495Cadmium acetate, dihydrate촉매HCID 2631-Butanol용매

실험 절차

10.9 g (60 mmoles) of undecyl cyanide was treated with 5 g (66.6 mmoles) of DL-2-amino-1-propanol in presence of 400 mg (1.5 mmoles) of cadmium acetate dihydrate in 1-butanol as outlined under Example 1. 13.2 g (92%) of product was obtained on distillation at 115°-117° C./1-1.5 mm Hg.

출처 및 근거

ORD 기록
ord-8fcaecc793d94a60abd145079f17f86a
출처 데이터셋
uspto-grants-1991_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05030629

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