Hydrochloric Acid → HCID 19807226, 화합물

반응식

[CH3:1][C:2]1[CH:13]=[CH:12][CH:11]=[C:10]2[C:3]=1[NH:4][CH:5]=[C:6]2[CH2:7][CH2:8][NH2:9].[C:14](O)(=O)C=O.[ClH:19]>>[ClH:19].[CH3:1][C:2]1[CH:13]=[CH:12][CH:11]=[C:10]2[C:3]=1[NH:4][C:5]1[CH2:14][NH:9][CH2:8][CH2:7][C:6]2=1

참가 물질

반응물 3

HCID 313Hydrochloric Acid

HCID 760Glyoxylic Acid

HCID 267147-Methyltryptamine

생성물 1

HCID 19807226HCID 19807226, 화합물

실험 절차

7-Methyltryptamine (free base, Sigma) was dissolved in aqueous hydrochloric acid and condensed with glyoxylic acid as described in part B. The product was decarboxylated according to part C to yield 8-methyl-1,2,3,4-tetrahydro-beta-carboline hydrochloride, which was recrystallized from ethanol:water R1-7 =R9 =H; R8 =Me).

출처 및 근거

ORD 기록: ord-0c66309870014f0cb7ccac5a7ac4d146
출처 데이터셋: uspto-grants-1990_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04978669

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