(+-)-p-Methoxyamphetamine → HCID 20434113, 화합물

HRID 1154605

반응식

HRID 1154605 반응식
[OH2:1].[CH2:2]([O:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[C:16]([CH:18]=O)=O)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH3:20][CH:21]([NH2:31])[CH2:22][C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1>CS(C)=O>[CH3:20][CH:21]([N:31]=[C:10]([O:9][CH2:2][C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1)[C:15]([C:14]1[CH:13]=[CH:12][CH:11]=[CH:16][CH:18]=1)=[O:1])[CH2:22][C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1

참가 물질

4

반응물 2

HCID 31721(+-)-p-MethoxyamphetamineHCID 204340852-Benzyloxyphenylglyoxal hydrate

생성물 1

HCID 20434113HCID 20434113, 화합물

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매2회

실험 절차

3.08 g of 2-benzyloxyphenylglyoxal hydrate (crude oil) are dissolved in 10 ml of dimethylsulfoxide, and 2.1 g of α-methyl-4-methoxyphenethylamine are added thereto. The mixture is stirred at room temperature for 45 minutes, whereby a solution of α-(α-methyl-4-methoxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.

출처 및 근거

ORD 기록
ord-ba214585f48e496585b1c94fe26ae302
출처 데이터셋
uspto-grants-1984_12
특허 번호
US04490392

연결된 노트

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