Dimethyl Sulfoxide → HCID 20434109, 화합물

HRID 1154616

반응식

HRID 1154616 반응식
O.CO[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]([CH:12]=[O:13])=[O:11].[CH3:14][CH:15]([NH2:25])[CH2:16][C:17]1[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][CH:18]=1.[CH3:26]S(C)=O>>[CH3:14][CH:15]([N:25]=[C:12]([O:13][CH3:26])[C:10]([C:5]1[CH:4]=[CH:9][CH:8]=[CH:7][CH:6]=1)=[O:11])[CH2:16][C:17]1[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][CH:18]=1

참가 물질

4

반응물 3

HCID 679Dimethyl Sulfoxide2회HCID 31721(+-)-p-MethoxyamphetamineHCID 204341102-Methoxyphenylglyoxal hydrate

생성물 1

HCID 20434109HCID 20434109, 화합물

실험 절차

2.9 g of 2-methoxyphenylglyoxal hydrate (crude oil) are dissolved in 6 ml of dimethylsulfoxide, and 2 g of α-methyl-4-methoxyphenethylamine are added thereto. The mixture is treated in the same manner as described in Example 1-(2), whereby a solution of α-(α-methyl-4-methoxyphenethylimino)-2-methoxyacetophenone in dimethylsulfoxide is obtained.

후처리

  1. additionThe mixture is treated in the same manner

출처 및 근거

ORD 기록
ord-0932d662c2e9447a9a8418898ede9ca9
출처 데이터셋
uspto-grants-1984_12
특허 번호
US04490392

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