Azobisisobutyronitrile → Styrene glycidyl Methacrylate

HRID 1166408

반응식

HRID 1166408 반응식
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9]([O:14][CH2:15][CH:16]1[O:18][CH2:17]1)(=[O:13])[C:10]([CH3:12])=[CH2:11].N(C(C)(C)C#N)=NC(C)(C)C#N>C1(C)C=CC=CC=1>[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9]([O:14][CH2:15][CH:16]1[O:18][CH2:17]1)(=[O:13])[C:10]([CH3:12])=[CH2:11]

참가 물질

5

반응물 3

HCID 6547AzobisisobutyronitrileHCID 7501StyreneHCID 7837Glycidyl methacrylate

생성물 1

HCID 21867792Styrene glycidyl Methacrylate

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

The same four-necked flask as used in Example 1 was charged with 100 g of toluene, and the temperature was adjusted to 80° C. with stirring under nitrogen. Then, 120 g of styrene, 89 g of glycidyl methacrylate and 0.1 g of azobisisobutyronitrile were added thereto and the reaction carried out in the same manner as in Example 1 to give a styrene-glycidyl methacrylate copolymer. This copolymer (96 weight parts) and 4 weight parts of 4,4′-bisazidobenzal(4-methyl)cyclohexanone were dissolved in 100 weight parts of xylene and the solution was subjected to polymerization in the same manner as in Example 1, whereupon an over coat film was obtained.

후처리

  1. customwas adjusted to 80° C.

출처 및 근거

ORD 기록
ord-a6513315a0884485aafab8d4df47f1db
출처 데이터셋
uspto-grants-2003_09
특허 번호
US06613855B1

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