Gamma-undecalactone → Sodium 4-hydroxyundecanoate
반응식
[OH-:1].[Na+:2].[CH3:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH:10]1[O:15][C:13](=[O:14])[CH2:12][CH2:11]1>CO>[Na+:2].[OH:15][CH:10]([CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH3:3])[CH2:11][CH2:12][C:13]([O-:14])=[O:1]참가 물질
4
실험 절차
To a solution of 43.6 g sodium hydroxide in 150 ml of methanol heated to reflux, 200 g gamma-undecalactone were added. After stirring for 2 hours at reflux, the mixture was cooled to room temperature and evaporated to dryness. The resulting crystals were washed with hexane to yield 240 g of colorless crystals.
후처리
- temperatureto reflux
- temperatureat reflux
- customevaporated to dryness
- washThe resulting crystals were washed with hexane
출처 및 근거
- ORD 기록
- ord-24fa95b31a2d4bca92e2c6895991a30d
- 출처 데이터셋
- uspto-grants-2003_09
- 특허 번호
- US06627763B2
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