Benzoyl chloride → 4-Methoxybenzophenone

HRID 1180324

반응식

HRID 1180324 반응식
[C:1]1([O:7][CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:9](Cl)(=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.B12B3B4B1C234>C1C=CC=CC=1>[CH3:8][O:7][C:1]1[CH:6]=[CH:5][C:4]([C:9](=[O:16])[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:3][CH:2]=1

참가 물질

5

반응물 3

HCID 7412Benzoyl chlorideHCID 7519AnisoleHCID 123279Boron carbide

생성물 1

HCID 691464-Methoxybenzophenone수율 48.2%

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

A mixture of 5.4 gm (0.05 moles) of anisole and 7.0 gm (0.05) moles of benzoyl chloride and 0.5 gm of boron carbide was placed in 50 ml of benzene. This mixture was allowed to react as described in Example 3. A yield of 48.2% of p-methoxy benzophenone was obtained, and 0.5 gm of the boron carbide catalysts was recovered.

후처리

  1. customto react

출처 및 근거

ORD 기록
ord-1185fc3e6a64469d9b8dbfeb70c90873
출처 데이터셋
uspto-grants-2007_10
특허 번호
US07279604B2

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