Dicyclohexylcarbodiimide → Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester
반응식
[CH2:1]([O:3][C:4](=[O:8])[CH2:5][O:6][NH2:7])[CH3:2].[C:9](O)(=[O:14])[CH2:10][CH2:11][C:12]#[CH:13].C1(N=C=NC2CCCCC2)CCCCC1>CCOC(C)=O>[CH2:1]([O:3][C:4](=[O:8])[CH2:5][O:6][NH:7][C:9](=[O:14])[CH2:10][CH2:11][C:12]#[CH:13])[CH3:2]참가 물질
5
실험 절차
To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.
출처 및 근거
- ORD 기록
- ord-128be03e30fc479198b6496eaff8785b
- 출처 데이터셋
- uspto-grants-2010_06
- 특허 번호
- US07727713B2
반응 노트
불러오는 중…