Dicyclohexylcarbodiimide → Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester

HRID 12009

반응식

HRID 12009 반응식
[CH2:1]([O:3][C:4](=[O:8])[CH2:5][O:6][NH2:7])[CH3:2].[C:9](O)(=[O:14])[CH2:10][CH2:11][C:12]#[CH:13].C1(N=C=NC2CCCCC2)CCCCC1>CCOC(C)=O>[CH2:1]([O:3][C:4](=[O:8])[CH2:5][O:6][NH:7][C:9](=[O:14])[CH2:10][CH2:11][C:12]#[CH:13])[CH3:2]

참가 물질

5

반응물 3

HCID 10868DicyclohexylcarbodiimideHCID 198082-Aminoxy-acetic acid ethyl esterHCID 224644-Pentynoic acid

생성물 1

HCID 59336531Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.

출처 및 근거

ORD 기록
ord-128be03e30fc479198b6496eaff8785b
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07727713B2

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