2,3-Diaminotoluene → HCID 178494311, 화합물
반응식
[Cl:1][C:2]1[N:7]=[N:6][C:5]([O:8][CH3:9])=[C:4]([CH:10]=O)[CH:3]=1.[NH2:12][C:13]1[C:18]([NH2:19])=[CH:17][CH:16]=[CH:15][C:14]=1[CH3:20]>CN(C=O)C>[Cl:1][C:2]1[N:7]=[N:6][C:5]([O:8][CH3:9])=[C:4]([C:10]2[NH:12][C:13]3[C:14]([CH3:20])=[CH:15][CH:16]=[CH:17][C:18]=3[N:19]=2)[CH:3]=1참가 물질
4
반응 조건
- 온도
- 120 °C
실험 절차
6-Chloro-3-methoxypyridazine-4-carbaldehyde is dissolved in DMF, und 2,3-diaminotoluene is added. The reaction solution is heated at 120° C. in a microwave for 30 minutes. The crude product is purified on silica gel (eluent ethyl acetate in heptane). MS (ES+) m/z 275 (M+H).
후처리
- customThe crude product is purified on silica gel (eluent ethyl acetate in heptane)
출처 및 근거
- ORD 기록
- ord-e986e39eba024f0d9b164fdcba6d54bc
- 출처 데이터셋
- uspto-grants-2010_06
- 특허 번호
- US07727989B2
반응 노트
불러오는 중…