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Iodoethane → 2-(Ethylthio)-5-methoxypyrimidine-4,6(1H,5H)-dione

HRID 1245422
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HRID 1245422 반응식
[CH2:1](I)[CH3:2].[CH3:4][O:5][CH:6]1[C:11](=[O:12])[NH:10][C:9](=[S:13])[NH:8][C:7]1=[O:14].[OH-].[Na+]>O>[CH2:1]([S:13][C:9]1[NH:8][C:7](=[O:14])[CH:6]([O:5][CH3:4])[C:11](=[O:12])[N:10]=1)[CH3:2]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 6340IodoethaneHCID 14798Sodium HydroxideHCID 219124765-Methoxy-2-thioxodihydropyrimidine-4,6(1H,5H)-dione

생성물 1

HCID 219124642-(Ethylthio)-5-methoxypyrimidine-4,6(1H,5H)-dione

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Ethyl iodide (11.2 ml) was added dropwise to a stirred mixture of the product from step (i) (23 g) and sodium hydroxide (6 g) in water (400 ml). After 16 h the mixture was filtered, the filtrate acidified to pH1 and the precipitate filtered, washed with water and dried. Yield 17.8 g

후처리

  1. filtrationAfter 16 h the mixture was filtered
  2. filtrationthe precipitate filtered
  3. washwashed with water
  4. customdried

출처 및 근거

ORD 기록
ord-7e54e2529ee5435eba8ed70b5e3726f1
출처 데이터셋
uspto-grants-2006_10
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07125881B2

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