2,4-Dichlorobenzoyl chloride → HCID 178496933, 화합물

HRID 1248347

반응식

HRID 1248347 반응식
[Cl-].[Cl-].[Cl-].[Al+3].[CH3:5][O:6][C:7]([C:9]1[C:12]2[CH:13]=[C:14]([O:17]C)[CH:15]=[CH:16][C:11]=2[CH:10]=1)=[O:8].[Cl:19][C:20]1[CH:28]=[C:27]([Cl:29])[CH:26]=[CH:25][C:21]=1[C:22](Cl)=[O:23]>>[CH3:5][O:6][C:7]([C:9]1[C:12]2[CH:13]=[C:14]([OH:17])[C:15]([C:22](=[O:23])[C:21]3[CH:25]=[CH:26][C:27]([Cl:29])=[CH:28][C:20]=3[Cl:19])=[CH:16][C:11]=2[CH:10]=1)=[O:8]

참가 물질

4

반응물 3

HCID 666452,4-Dichlorobenzoyl chlorideHCID 6451240Aluminum(III) ChlorideHCID 541184135-Methoxybenzocyclobutene-1-carboxylic acid methyl ester

생성물 1

HCID 178496933HCID 178496933, 화합물

실험 절차

In a manner analogous to that described in Example 5, starting from 26.6 g of aluminium trichloride, 9.61 g of 5-methoxybenzocyclobutene-1-carboxylic acid methyl ester and 20.95 g of 2,4-dichlorobenzoyl chloride there is obtained 4-(2,4-dichlorobenzoyl)-5-hydroxybenzocyclobutene-1-carboxylic acid methyl ester having a melting point of 99°-100°.

출처 및 근거

ORD 기록
ord-fbea0220bd6b49d5837f15bd072fe64a
출처 데이터셋
uspto-grants-1985_06
특허 번호
US04523030

연결된 노트

불러오는 중…