Sodium Hydroxide → 2,3-Dihydro-thieno(3,4-b)(1,4)dioxin-5,7-dicarboxylic acid

HRID 1257130

반응식

HRID 1257130 반응식
C([O:3][C:4]([C:6]1[S:7][C:8]([C:15]([O:17]CC)=[O:16])=[C:9]2[O:14][CH2:13][CH2:12][O:11][C:10]=12)=[O:5])C.[OH-].[Na+]>>[C:15]([C:8]1[S:7][C:6]([C:4]([OH:5])=[O:3])=[C:10]2[O:11][CH2:12][CH2:13][O:14][C:9]=12)([OH:17])=[O:16]

참가 물질

3

반응물 2

HCID 14798Sodium HydroxideHCID 625399Diethyl 2,3-dihydrothieno[3,4-b][1,4]dioxine-5,7-dicarboxylate

생성물 1

HCID 7288412,3-Dihydro-thieno(3,4-b)(1,4)dioxin-5,7-dicarboxylic acid

실험 절차

The 2,5-diethoxycarbonyl-3,4-ethylenedioxythiophene and NaOH are mixed in the microwave reactor. The microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W to perform hydrolysis reaction for no more than 20 minutes to obtain 2,5-dicarboxy-3,4-ethylenedioxythiophene.

후처리

  1. temperatureThe microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W
  2. customhydrolysis reaction for no more than 20 minutes

출처 및 근거

ORD 기록
ord-211382df869c46338f0100cc3b539058
출처 데이터셋
uspto-grants-2013_06
특허 번호
US08461355B2

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