Methanol → 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine

HRID 1266730

반응식

HRID 1266730 반응식
Cl[C:2]1[C:3]([N:12]2[CH:16]=[CH:15][CH:14]=[CH:13]2)=[CH:4][C:5]([N+:9]([O-:11])=[O:10])=[C:6]([NH2:8])[CH:7]=1.[CH3:17][OH:18].[OH-].[K+]>CS(C)=O>[CH3:17][O:18][C:2]1[C:3]([N:12]2[CH:16]=[CH:15][CH:14]=[CH:13]2)=[CH:4][C:5]([N+:9]([O-:11])=[O:10])=[C:6]([NH2:8])[CH:7]=1

참가 물질

5

반응물 3

HCID 887MethanolHCID 14797Potassium HydroxideHCID 185488595-Chloro-2-nitro-4-pyrrol-1-yl-phenylamine

생성물 1

HCID 185487175-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매

실험 절차

The title compound was prepared from 5-chloro-2-nitro-4-pyrrol-1-yl-phenylamine (Example F3) (5.94 g, 25 mmol), methanol (25 mL) and KOH (1.98 g, 30 mmol) in DMSO (25 mL) according to the general procedure E. Obtained as an orange solid (5.88 g).

출처 및 근거

ORD 기록
ord-e6ee15db5ebc44d9980b62679a2b0bb5
출처 데이터셋
uspto-grants-2003_04
특허 번호
US06548495B2

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