Hydrochloric Acid → Sodium Dilysine Succinate Hydrochloride

HRID 128508

반응식

HRID 128508 반응식
O.[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[C:12]([O-:19])(=[O:18])[CH2:13][CH2:14][C:15]([O-:17])=[O:16].[Na+:20].[Na+].C(O)(=O)CCC(O)=O.[ClH:30]>O>[ClH:30].[C:12]([O-:19])(=[O:18])[CH2:13][CH2:14][C:15]([O-:17])=[O:16].[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[Na+:20].[Na+:20]

참가 물질

6

반응물 4

HCID 313Hydrochloric Acid2회HCID 1110Succinic AcidHCID 9020Sodium SuccinateHCID 16211825Lysine Monohydrate

생성물 1

HCID 86749085Sodium Dilysine Succinate Hydrochloride

시약·촉매·용매 1

HCID 962Water용매

실험 절차

12 grams of L-lysine monohydrate is dissolved in 20 ml of water to which 6.0 ml of concentrated hydrochloric acid has been added. 2.964 grams of disodium succinate is added to neutralize some of the excess hydrochloric acid and 2.16 grams of succinic acid are added with mixing until effervescence ceases and all solids are dissolved. The solution is dried in a 110° C. oven until solids begin to form when cooled to room temperature. After 15 to 30 minutes solids form and are collected.

후처리

  1. additionhas been added
  2. additionare added
  3. additionwith mixing until effervescence ceases
  4. dissolutionall solids are dissolved
  5. customThe solution is dried in a 110° C. oven until solids
  6. customto form when
  7. customare collected

출처 및 근거

ORD 기록
ord-aa57a6c4c6e742af843ffca8738af246
출처 데이터셋
uspto-grants-1995_11
특허 번호
US05464651

연결된 노트

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