1-Bromopropane → HCID 19374328, 화합물

HRID 128611노트

반응식

HRID 128611 반응식
[OH:1][C:2]1[C:3]([CH3:8])=[N:4][CH:5]=[CH:6][CH:7]=1.[Na].Br[CH2:11][CH2:12][CH3:13]>C(O)CC>[CH3:8][C:3]1[C:2]([O:1][CH2:11][CH2:12][CH3:13])=[CH:7][CH:6]=[CH:5][N:4]=1

참가 물질

5

반응물 3

HCID 78401-BromopropaneHCID 707192-Methylpyridin-3-olHCID 5360545Sodium

생성물 1

HCID 19374328HCID 19374328, 화합물

시약·촉매·용매 1

HCID 10311-Propanol용매2회

실험 절차

3-Hydroxy-2-methylpyridine (50 g) was added to a solution of sodium (11.6 g) in propan-1-ol (250 ml) and the mixture treated with 1-bromopropane (51 ml) in propan-1-ol (50 ml) to give 2-methyl-3-propoxypyridine, b.p. 96°-104° C. (30 mmHg).

출처 및 근거

ORD 기록
ord-9e6b084079f44c2d845926ea4abf4213
출처 데이터셋
uspto-grants-1995_11
특허 번호
US05464781

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