3-Bromopyridine → Biphenyl

HRID 1286117

반응식

HRID 1286117 반응식
Brc1cccnc1.N=C(N)Cc1ccccc1>CN1CCCN2CCCN=C12.CS(=O)(=O)[O][Pd]1(<-[NH2]c2ccccc2-c2cccc[c]21)<-[P](c1ccccc1)(c1ccccc1)c1ccc2ccccc2c1-c1c(P(c2ccccc2)c2ccccc2)ccc2ccccc12.CS(C)=O>N=C(Cc1ccccc1)Nc1cccnc1

참가 물질

9

반응물 2

HCID 122863-BromopyridineHCID 27787Benzeneethanimidamide

생성물 4

HCID 7095BiphenylHCID 122863-BromopyridineHCID 27787BenzeneethanimidamideHCID 178510790HCID 178510790, 화합물

시약·촉매·용매 3

HCID 1235837-Methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene시약HCID 178505363HCID 178505363, 화합물시약HCID 679Dimethyl Sulfoxide용매4회

실험 절차

The Mosquito was used to combine the source plate solutions by multi-aspiration of 250 nL of each of the four reaction components and then to dose the resulting reaction mixture (1 uL) into a 1536-well plate

후처리

  1. addition기록된 절차가 없습니다
  2. aliquot기록된 절차가 없습니다
  3. addition기록된 절차가 없습니다

출처 및 근거

ORD 기록
ord-fee82f2144f244d1bf8e67e55457f8eb
출처 데이터셋
HTE Pd-catalyzed cross-coupling screen
원본 링크
출처 보기

연결된 노트

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