1H-Indazole → Biphenyl

HRID 1286308노트

반응식

HRID 1286308 반응식
Brc1cccnc1.c1ccc2[nH]ncc2c1>C1CCC2=NCCCN2CC1.CS(=O)(=O)[O][Pd]1(<-[NH2]c2ccccc2-c2cccc[c]21)<-[P](c1ccccc1)(c1ccccc1)c1ccc2ccccc2c1-c1c(P(c2ccccc2)c2ccccc2)ccc2ccccc12.CS(C)=O>c1cncc(-n2ncc3ccccc32)c1

참가 물질

9

반응물 2

HCID 92211H-IndazoleHCID 122863-Bromopyridine

생성물 4

HCID 7095BiphenylHCID 92211H-IndazoleHCID 122863-BromopyridineHCID 113560351H-Indazole, 1-(3-pyridinyl)-

시약·촉매·용매 3

HCID 811841,8-Diazabicyclo(5.4.0)undec-7-ene시약HCID 178505363HCID 178505363, 화합물시약HCID 679Dimethyl Sulfoxide용매4회

실험 절차

The Mosquito was used to combine the source plate solutions by multi-aspiration of 250 nL of each of the four reaction components and then to dose the resulting reaction mixture (1 uL) into a 1536-well plate

후처리

  1. addition기록된 절차가 없습니다
  2. aliquot기록된 절차가 없습니다
  3. addition기록된 절차가 없습니다

출처 및 근거

ORD 기록
ord-8dc24d7cf8434a308f8409e2a10c4f10
출처 데이터셋
HTE Pd-catalyzed cross-coupling screen
원본 링크
출처 보기

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