1H-Indazole → Biphenyl

HRID 1286315노트

반응식

HRID 1286315 반응식
Brc1cccnc1.c1ccc2[nH]ncc2c1>CN1CCCN2CCCN=C12.CS(=O)(=O)[O][Pd]1(<-[NH2]c2ccccc2-c2cccc[c]21)<-[P](C1=CC=C[CH]1[Fe][CH]1C=CC=C1P(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.CS(C)=O>c1cncc(-n2ncc3ccccc32)c1

참가 물질

9

반응물 2

HCID 92211H-IndazoleHCID 122863-Bromopyridine

생성물 4

HCID 7095BiphenylHCID 92211H-IndazoleHCID 122863-BromopyridineHCID 113560351H-Indazole, 1-(3-pyridinyl)-

시약·촉매·용매 3

HCID 1235837-Methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene시약HCID 178505365HCID 178505365, 화합물시약HCID 679Dimethyl Sulfoxide용매4회

실험 절차

The Mosquito was used to combine the source plate solutions by multi-aspiration of 250 nL of each of the four reaction components and then to dose the resulting reaction mixture (1 uL) into a 1536-well plate

후처리

  1. addition기록된 절차가 없습니다
  2. aliquot기록된 절차가 없습니다
  3. addition기록된 절차가 없습니다

출처 및 근거

ORD 기록
ord-2901cf0a0bcf4390ad02bf10a9e58ac0
출처 데이터셋
HTE Pd-catalyzed cross-coupling screen
원본 링크
출처 보기

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